饮用水检测
近日曝出某桶装水砷汞含量超标，汪老师送检了几份水样，大家可以参考：
首先是饮用水的毒理指标（就是超过就说明不好了）
净化水（用家用过滤饮水机制备）
File Name : 净化水
File Path : D:\DATA\20130418\WANG-1.D\
Method : d:\ICPCHEM\1\METHODS\heavyM.M
Calibration : D:\ICPCHEM\1\CALIB\heavyM.C
Acq Time : Apr 18 2013 03:11 pm
Sample Name : wanghong -1
Sample Type : Sample
Comments :
Prep Dilution : 1.000
Auto Dilution : Undiluted
Total Dilution : 1.000
Operator Name:
Acq Mode : Spectrum
Cal Title :
Cal Type : External Calibration Method
Last Calib : Apr 18 2013 03:52 pm
Bkg File : ——–
Bkg Rejected Masses: ——–
Interference Correction : ON
Blank File : ——–
VIS Fit : Point to Point
Weighting Method: 1/(SD*SD)
Element Mass ISTD CPS or Ratio Conc. RSD(%) Time(sec) Rep VIS
含量
Cr 52 103 0.1123416 P 4.769E-01 ppb 6.24 0.60 3
As 75 103 0.01083997 P 5.115E-02 ppb 746.63 0.60 3
Se 77 103 0.003229336 P 3.743 ppb 22.14 0.60 3
Rh 103 330,324.5 P [ 1.000 ] --- 0.60 [ 3 ]
Cd 111 103 0.002823968 P 2.939E-01 ppb 111.70 0.60 3
Hg 202 103 0.2929443 P 9.329 ppb 27.15 0.60 3
Pb 208 103 0.08932206 P 5.634E-01 ppb 70.55 0.60 3
End of Report
Thu Apr 18 15:52:42 2013
某瓶装水一
File Name : 鸟窝瓶装水
File Path : D:\DATA\20130418\WANG-2.D\
Method : d:\ICPCHEM\1\METHODS\heavyM.M
Calibration : D:\ICPCHEM\1\CALIB\heavyM.C
Acq Time : Apr 18 2013 03:15 pm
Sample Name : wanghong -2
Sample Type : Sample
Comments :
Prep Dilution : 1.000
Auto Dilution : Undiluted
Total Dilution : 1.000
Operator Name:
Acq Mode : Spectrum
Cal Title :
Cal Type : External Calibration Method
Last Calib : Apr 18 2013 03:54 pm
Bkg File : ——–
Bkg Rejected Masses: ——–
Interference Correction : ON
Blank File : ——–
VIS Fit : Point to Point
Weighting Method: 1/(SD*SD)
Element Mass ISTD CPS or Ratio Conc. RSD(%) Time(sec) Rep VIS
含量
Cr 52 103 0.1529895 P 5.064E-01 ppb 0.68 0.60 3
As 75 103 0.006445185 P <0.000 ppb 14.70 0.60 3
Se 82 103 0.002200148 P 8.461E-01 ppb 19.23 0.60 3
Cd 111 103 8.199484E-4 P 1.109E-02 ppb 417.67 0.60 3
Hg 202 103 0.2412668 P 2.816 ppb 13.66 0.60 3
Pb 208 103 0.02101727 P <0.000 ppb 16.45 0.60 3
End of Report
Thu Apr 18 15:54:09 2013
小桶泉水
File Name : 小桶泉水
File Path : D:\DATA\20130418\WANG-3.D\
Method : d:\ICPCHEM\1\METHODS\heavyM.M
Calibration : D:\ICPCHEM\1\CALIB\heavyM.C
Acq Time : Apr 18 2013 03:19 pm
Sample Name : wanghong -3
Sample Type : Sample
Comments :
Prep Dilution : 1.000
Auto Dilution : Undiluted
Total Dilution : 1.000
Operator Name:
Acq Mode : Spectrum
Cal Title :
Cal Type : External Calibration Method
Last Calib : Apr 18 2013 03:56 pm
Bkg File : ——–
Bkg Rejected Masses: ——–
Interference Correction : ON
Blank File : ——–
VIS Fit : Point to Point
Weighting Method: 1/(SD*SD)
-
Element Mass ISTD CPS or Ratio Conc. RSD(%) Time(sec) Rep VIS
含量
Cr 52 103 0.1553680 P 5.081E-01 ppb 0.77 0.60 3
As 75 103 0.01290261 P 2.849E-01 ppb 38.96 0.60 3
Se 82 103 0.001937876 P 4.564E-01 ppb 67.05 0.60 3
Cd 111 103 6.913544E-4 P <0.000 ppb 105.59 0.60 3
Hg 202 103 0.2539830 P 4.418 ppb 15.02 0.60 3
Pb 208 103 0.02037368 P <0.000 ppb 3.04 0.60 3
End of Report
Thu Apr 18 15:56:01 2013
大桶泉水
File Name :大桶泉水
File Path : D:\DATA\20130418\WANG-4.D\
Method : d:\ICPCHEM\1\METHODS\heavyM.M
Calibration : D:\ICPCHEM\1\CALIB\heavyM.C
Acq Time : Apr 18 2013 03:22 pm
Sample Name : wanghong -4
Sample Type : Sample
Comments :
Prep Dilution : 1.000
Auto Dilution : Undiluted
Total Dilution : 1.000
Operator Name:
Acq Mode : Spectrum
Cal Title :
Cal Type : External Calibration Method
Last Calib : Apr 18 2013 03:56 pm
Bkg File : ——–
Bkg Rejected Masses: ——–
Interference Correction : ON
Blank File : ——–
VIS Fit : Point to Point
Weighting Method: 1/(SD*SD)
Element Mass ISTD CPS or Ratio Conc. RSD(%) Time(sec) Rep VIS
含量
Cr 52 103 0.1398022 P 4.968E-01 ppb 0.49 0.60 3
As 75 103 0.01379683 P 3.862E-01 ppb 5.43 0.60 3
Se 82 103 0.001609006 P <0.000 ppb 236.17 0.60 3
Cd 111 103 5.888494E-4 P <0.000 ppb 28.22 0.60 3
Hg 202 103 0.2165745 P <0.000 ppb 72.06 0.60 3
Pb 208 103 0.01765149 P <0.000 ppb 1.36 0.60 3
End of Report
Thu Apr 18 15:56:48 2013